Event Title

Preparation of some new Aryl Diethyl Phosphate and their use in Metal- Catalyzed Reaction

Location

CSU 253/4/5

Start Date

4-4-2011 11:00 AM

End Date

4-4-2011 12:30 PM

Student's Major

Chemistry and Geology

Student's College

Science, Engineering and Technology

Mentor's Name

Michael Lusch

Mentor's Department

Chemistry and Geology

Mentor's College

Science, Engineering and Technology

Description

The Characterization of this compound was carried out by proton (1H) and Carbon -13 NMR (Nuclear magnetic Resonance Spectroscopy), Infrared Spectroscopy, and mass spectroscopy. The overall research experiment was to make a compound that had not being made in the MSU organic Chemistry Department. This experiment was carried out by following the procedure of Kenner and Williams (H.W Kenner & N.R Williams, J. Chem. Soc 1955, PG 522-525.) This procedure instiu preparation of Chloro-diethyl-phosphate reacting with phenol under basic conditions to make corresponding aryl-diethyl-phosphate. The compound was purified by using flash chromatography. It structure was confirmed by NMRIR mass spectrometry. Once prepared these compound were subjected to middle catalyzed reaction.

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Apr 4th, 11:00 AM Apr 4th, 12:30 PM

Preparation of some new Aryl Diethyl Phosphate and their use in Metal- Catalyzed Reaction

CSU 253/4/5

The Characterization of this compound was carried out by proton (1H) and Carbon -13 NMR (Nuclear magnetic Resonance Spectroscopy), Infrared Spectroscopy, and mass spectroscopy. The overall research experiment was to make a compound that had not being made in the MSU organic Chemistry Department. This experiment was carried out by following the procedure of Kenner and Williams (H.W Kenner & N.R Williams, J. Chem. Soc 1955, PG 522-525.) This procedure instiu preparation of Chloro-diethyl-phosphate reacting with phenol under basic conditions to make corresponding aryl-diethyl-phosphate. The compound was purified by using flash chromatography. It structure was confirmed by NMRIR mass spectrometry. Once prepared these compound were subjected to middle catalyzed reaction.

Recommended Citation

Asamou, Emmanuel. "Preparation of some new Aryl Diethyl Phosphate and their use in Metal- Catalyzed Reaction." Undergraduate Research Symposium, Mankato, MN, April 4, 2011.
http://cornerstone.lib.mnsu.edu/urs/2011/poster-session-B/11