Synthesis of 5-[5-(5-Formyi-2-thienyI)-2-furyl]-2-thiophenecarbaIdehyde
Location
CSU 255A/B
Start Date
23-4-2007 10:00 AM
End Date
23-4-2007 12:00 PM
Student's Major
Chemistry and Geology
Student's College
Science, Engineering and Technology
Mentor's Name
Brian L. Groh
Mentor's Department
Chemistry and Geology
Mentor's College
Science, Engineering and Technology
Description
5-[5-(5-Formyl-2-thienyl)-2-furyl]-2-thiophenecarbaldehyde (NSC 629035) has been found to possess antitumor properties in the NCI Anticancer Drug Screen. A similar compound, 2,5-bis(5-hydroxymethyl-2- thienyl)furan (NSC 652287), has also been found to possess anti-tumor properties. A correlation between the ability to metabolize NSC 652287, hypothesized as NSC 629035, and its cytotoxicity has been demonstrated. The mechanism by which these compounds act is not fully understood. Approximately 3 g of commercially available NSC 629035 ($3,850/250 mg) is required for mechanistic studies. The prohibitive cost demanded the development of a viable synthetic approach to this compound. Two routes for the synthesis of NSC 629035 will be presented.
Synthesis of 5-[5-(5-Formyi-2-thienyI)-2-furyl]-2-thiophenecarbaIdehyde
CSU 255A/B
5-[5-(5-Formyl-2-thienyl)-2-furyl]-2-thiophenecarbaldehyde (NSC 629035) has been found to possess antitumor properties in the NCI Anticancer Drug Screen. A similar compound, 2,5-bis(5-hydroxymethyl-2- thienyl)furan (NSC 652287), has also been found to possess anti-tumor properties. A correlation between the ability to metabolize NSC 652287, hypothesized as NSC 629035, and its cytotoxicity has been demonstrated. The mechanism by which these compounds act is not fully understood. Approximately 3 g of commercially available NSC 629035 ($3,850/250 mg) is required for mechanistic studies. The prohibitive cost demanded the development of a viable synthetic approach to this compound. Two routes for the synthesis of NSC 629035 will be presented.
Recommended Citation
Bequette, Joseph P.. "Synthesis of 5-[5-(5-Formyi-2-thienyI)-2-furyl]-2-thiophenecarbaIdehyde." Undergraduate Research Symposium, Mankato, MN, April 23, 2007.
https://cornerstone.lib.mnsu.edu/urs/2007/oral-session-05/3